Journal of Chemical and Pharmaceutical Research (ISSN : 0975-7384)

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Original Articles: 2015 Vol: 7 Issue: 2

Determination of Giazepam Aminobenzophenones by two Ã?¢Ã?â?¬Ã?â??dimensional gas chromatography-mass spectrometry (GC-GC-MS) in urine

Abstract

In this study, an evaluation of suitable extraction and clean up techniques for benzophenones of gidazepam in urine samples was done. Solvent extraction methods were compared with solid-phase extraction using Bond Elut Certify. For end-step detection method two–dimensional gas chromatography-mass spectrometry (GC-GC/MS) were evaluated. Presence of aminocarboxibromobenzophenone in the urine was an indicator of the subject being a probable abuser of gidazepam.

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